Development of a fluidic cell to image precipitation reactions by x-ray microscopy

Charlie Gosse (1) , Joni Frederick (2) , Christian Blot (2) , Stephane Lefrancois (3) , Sufal Swaraj (3) , Stefan Stanescu (3) , Rachid Belkhou (3) , Patrick Guenoun (2) , Corinne Chevallard (2)

1 LPN - Laboratoire de photonique et de nanostructures
2 LIONS - Laboratoire Interdisciplinaire sur l'Organisation Nanométrique et Supramoléculaire
3 SSOLEIL - Synchrotron SOLEIL

We introduce an observation chamber dedicated to image, at the nanoscale, the kinetics of reactions taking place at the liquid/solid interface. The assembly of this microfluidic cell is straightforward and, most importantly, its design allow the operator to precisely regulate the hydrodynamic flow and control the concentration in reagents at the observation window.

Keywords: Chemical kinetics; biomineralization; scanning transmission X-ray microscopy; in operando imaging; microreactor

Domains: Material chemistry

Charlie Gosse, Joni Frederick, Christian Blot, Stephane Lefrancois, Sufal Swaraj, et al.. Development of a fluidic cell to image precipitation reactions by x-ray microscopy. 2017 19th International Conference on Solid-State Sensors, Actuators and Microsystems (TRANSDUCERS), Jun 2017, Kaohsiung, Taiwan. pp.1734-1737, ⟨10.1109/TRANSDUCERS.2017.7994402⟩. ⟨cea-02368479⟩