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Evaluation of a high-resolution micro-sized magic angle spinning (HR[small mu ]MAS) probe for NMR-based metabolomic studies of nanoliter samples

Tuan Nghia Duong 1, 2 Yuki Endo 2 Takahiro Nemoto 2 Hiroshi Kato 2 Anne-Karine Bouzier-Sore 3 Yusuke Nishiyama 1, 2 Alan Wong 4
1 RIKEN CLST - RIKEN Center for Life Science Technologies
2 JEOL Ltd, 1156 Nakagami, Akishima, Tokyo 196-0022, Japan.
3 RMSB - Résonance magnétique des systèmes biologiques
4 LSDRM - Laboratoire Structure et Dynamique par Résonance Magnétique (LCF)
NIMBE UMR 3685 - Nanosciences et Innovation pour les Matériaux, la Biomédecine et l'Energie (ex SIS2M)
Abstract : This study evaluates the performances of a recently introduced 1 mm HR[small mu ]MAS NMR probe for metabolic profiling of nanoliter samples. It examines essential NMR criteria such as spectral data qualities and repeatability, and experimental practicality. The report also discusses the difficulties related to the sample preparation in HR[small mu ]MAS experiments and considers possible solutions and improvements.
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https://hal-cea.archives-ouvertes.fr/cea-01380672
Contributor : Serge Palacin <>
Submitted on : Thursday, October 13, 2016 - 12:18:31 PM
Last modification on : Thursday, July 1, 2021 - 4:44:51 PM

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CEA | CNRS | PUBNIMBE | IRAMIS-NIMBE | CEA-UPSAY | INC-CNRS | IRAMIS | GS-CHIMIE | GS-ENGINEERING | INSTITUT-SCIENCES-LUMIERE

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Tuan Nghia Duong, Yuki Endo, Takahiro Nemoto, Hiroshi Kato, Anne-Karine Bouzier-Sore, et al.. Evaluation of a high-resolution micro-sized magic angle spinning (HR[small mu ]MAS) probe for NMR-based metabolomic studies of nanoliter samples. Analytical Methods, Royal Society of Chemistry, 2016, 8, pp.6815-6820. ⟨10.1039/C6AY01654E⟩. ⟨cea-01380672⟩

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